Synthesis and Real Structure Group

Precision Electron Diffraction (PED)

Precision Electron Diffraction is the equivalent to Burger precision technique for XRD machines. In the electron precession technique, the electron beam is tilted and precessed along a conical surface, having a common axis with the TEM optical axis. As a result this technique has following advantages:

-more reflections in the reciprocal lattice are visible than in SAD patterns

-reflection diffracted intensity is much closer to the integrated intensity values

-the diffraction patterns can be considered more as kinematically images (like the images of a XRD machine) than dynamic ones.

In conclusion there are less disturbing influences and the interpretation of the images is much easier than for normal SAD images.



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